ASTM E1613 Standard Test Method for Determination of Lead by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES), Flame Atomic Absorption Spectrometry (FAAS), or Graphite Furnace Atomic Absorption Spectrometry (GFAAS) Techniques
ASTM E1613用感應耦合等離子體原子發射光譜法(ICP-AES),火焰原子吸收光譜法(FAAS)或石墨爐原子吸收光譜技術(GFAAS)測定鉛含量的標準試驗方法
This test method is intended for use with other standards (see 2.1) that address the collection and preparation of samples (dried chips, dusts, soils, and air particulates) that are obtained during the assessment or mitigation of lead hazards from buildings and related structures.
This test method may also be used to analyze similar samples from other environments.
1. Scope
1.1 This test method is intended for use with extracted or digested samples that were collected during the assessment, management, or abatement of lead hazards from buildings, structures, or other locations.
1.2 This test method covers the lead analysis of sample extracts or digestates (for example, extracted or digested paint, soil, dust, and airborne particulate) using inductively coupled plasma atomic emission spectrometry (ICP-AES), flame atomic absorption spectrometry (FAAS), or graphite furnace atomic absorption spectrometry (GFAAS).
1.3 This test method contains directions for sample analysis, as well as quality assurance (QA) and quality control (QC), and may be used for purposes of laboratory accreditation and certification.
1.4 No detailed operating instructions are provided because of differences among various makes and models of suitable instruments. Instead, the analyst shall follow the instructions provided by the manufacturer of the particular instrument.
1.5 The values stated in SI units are to be regarded as the standard.
1.6 This practice contains notes which are explanatory and not part of the mandatory requirements of this standard.
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents (purchase separately)
ASTM Standards
D1193 Specification for Reagent Water
D3919 Practice for Measuring Trace Elements in Water by Graphite Furnace Atomic Absorption Spectrophotometry
D4210 Practice for Intralaboratory Quality Control Procedures and a Discussion on Reporting Low-Level Data
D4697 Guide for Maintaining Test Methods in the Users Laboratory
D4840 Guide for Sampling Chain of Custody Procedures
D6785 Test Method for Determination of Lead in Workplace Air
E456 Terminology Relating to Quality and Statistics
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
E1188 Practice for Collection and Preservation of Information and Physical Items by a Technical Investigator
E1605 Terminology Relating to Abatement of Hazards from Lead-Based Paint in Buildings and Related Structures
E1644 Practice for Hot Plate Digestion of Dust Wipe Samples for Subsequent Determination of Lead by Atomic Spectrometry
E1645 Practice for Preparation of Dried Paint Samples for Subsequent Lead Analysis by Atomic Spectrometry
E1726 Practice for Sample Digestion of Soils for the Determination of Lead by Atomic Spectrometry
E1727 Practice for Field Collection of Soil Samples for Lead Determination by Atomic Spectrometry Techniques
E1728 Practice for Field Collection of Settled Dust Samples Using Wipe Sampling Methods for Lead Determination by Atomic Spectrometry Techniques
E1729 Practice for Field Collection of Dried Paint Samples for Determination by Atomic Spectrometry Techniques
E1741 Practice for Preparation of Airborne Particulate Lead Samples Collected During Abatement and Construction Activities for Subsequent Analysis by Atomic Spectrometry
E1775 Guide for Evaluating Performance of On-Site Extraction and Field-Portable Electrochemical or Spectrophotometric Analysis for Lead
E1792 Specification for Wipe Sampling Materials for Lead in Surface Dust
E1864 Practice for Evaluating Quality Systems of Organizations Engaged in Conducting Facility and Hazard Assessments to Determine the Presence and Extent of Lead in Paint, Dust, Airborne Particulate, and Soil in Buildings and Related Structures
E1973 Practice for Collection of Surface Dust by Air Sampling Pump Vacuum Technique for Subsequent Lead Determination
E1979 Practice for Ultrasonic Extraction of Paint, Dust, Soil, or Air Samples for Subsequent Determination of Lead
E2239 Practice for Record Keeping and Record Preservation for Lead Hazard Activities
Index Terms
GFAAS; ICP-AES; instrumental analysis; lead
ASTM E1613用感應耦合等離子體原子發射光譜法(ICP-AES),火焰原子吸收光譜法(FAAS)或石墨爐原子吸收光譜技術(GFAAS)測定鉛含量的標準試驗方法
This test method is intended for use with other standards (see 2.1) that address the collection and preparation of samples (dried chips, dusts, soils, and air particulates) that are obtained during the assessment or mitigation of lead hazards from buildings and related structures.
This test method may also be used to analyze similar samples from other environments.
1. Scope
1.1 This test method is intended for use with extracted or digested samples that were collected during the assessment, management, or abatement of lead hazards from buildings, structures, or other locations.
1.2 This test method covers the lead analysis of sample extracts or digestates (for example, extracted or digested paint, soil, dust, and airborne particulate) using inductively coupled plasma atomic emission spectrometry (ICP-AES), flame atomic absorption spectrometry (FAAS), or graphite furnace atomic absorption spectrometry (GFAAS).
1.3 This test method contains directions for sample analysis, as well as quality assurance (QA) and quality control (QC), and may be used for purposes of laboratory accreditation and certification.
1.4 No detailed operating instructions are provided because of differences among various makes and models of suitable instruments. Instead, the analyst shall follow the instructions provided by the manufacturer of the particular instrument.
1.5 The values stated in SI units are to be regarded as the standard.
1.6 This practice contains notes which are explanatory and not part of the mandatory requirements of this standard.
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents (purchase separately)
ASTM Standards
D1193 Specification for Reagent Water
D3919 Practice for Measuring Trace Elements in Water by Graphite Furnace Atomic Absorption Spectrophotometry
D4210 Practice for Intralaboratory Quality Control Procedures and a Discussion on Reporting Low-Level Data
D4697 Guide for Maintaining Test Methods in the Users Laboratory
D4840 Guide for Sampling Chain of Custody Procedures
D6785 Test Method for Determination of Lead in Workplace Air
E456 Terminology Relating to Quality and Statistics
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
E1188 Practice for Collection and Preservation of Information and Physical Items by a Technical Investigator
E1605 Terminology Relating to Abatement of Hazards from Lead-Based Paint in Buildings and Related Structures
E1644 Practice for Hot Plate Digestion of Dust Wipe Samples for Subsequent Determination of Lead by Atomic Spectrometry
E1645 Practice for Preparation of Dried Paint Samples for Subsequent Lead Analysis by Atomic Spectrometry
E1726 Practice for Sample Digestion of Soils for the Determination of Lead by Atomic Spectrometry
E1727 Practice for Field Collection of Soil Samples for Lead Determination by Atomic Spectrometry Techniques
E1728 Practice for Field Collection of Settled Dust Samples Using Wipe Sampling Methods for Lead Determination by Atomic Spectrometry Techniques
E1729 Practice for Field Collection of Dried Paint Samples for Determination by Atomic Spectrometry Techniques
E1741 Practice for Preparation of Airborne Particulate Lead Samples Collected During Abatement and Construction Activities for Subsequent Analysis by Atomic Spectrometry
E1775 Guide for Evaluating Performance of On-Site Extraction and Field-Portable Electrochemical or Spectrophotometric Analysis for Lead
E1792 Specification for Wipe Sampling Materials for Lead in Surface Dust
E1864 Practice for Evaluating Quality Systems of Organizations Engaged in Conducting Facility and Hazard Assessments to Determine the Presence and Extent of Lead in Paint, Dust, Airborne Particulate, and Soil in Buildings and Related Structures
E1973 Practice for Collection of Surface Dust by Air Sampling Pump Vacuum Technique for Subsequent Lead Determination
E1979 Practice for Ultrasonic Extraction of Paint, Dust, Soil, or Air Samples for Subsequent Determination of Lead
E2239 Practice for Record Keeping and Record Preservation for Lead Hazard Activities
Index Terms
GFAAS; ICP-AES; instrumental analysis; lead
